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- W2085829690 abstract "The methods of preparation of ReO3F are revised. ReO3F is an amorphous yellow solid that crystallizes into colorless needles after prolonged heating. Its structure is that of a fluorine and oxygen bridged chain with hexa coordinated rhenium atoms (a = 670.9(2), b = 596.6(2), c = 1030.6(4) pm, β = 90.057(7)°, space group P2/c. In presence of donor solvents ReO3F·2L (L = (C2H5)2O, (CH3)2O, THF) are formed. ReO2F3, if crystallized from HF, exists in two crystalline forms, both are fluorine bridged chain polymers. (ReO2F3-I: a = 1539.7(3), b = 999.6(3), c = 924.4(2) pm, β = 95.25(1)°, space group P21/c; ReO2F3-II: a = 544.9(1), b = 494.2(1), c = 1253.7(2) pm, β = 98.543(7)°, space group P21/c. ReO2F3 crystallizes from CFCl3 or SO2FCl as fluorine bridged cyclic trimer (a = 881.4(4), c = 822.1(6) pm, γ = 120°, space group P63/m, or fluorine bridged cyclic tetramer (a = 1107.8(2), b = 999.4(2), c = 1347.9(3) pm, space group Cmca)." @default.
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- W2085829690 date "2006-02-14" @default.
- W2085829690 modified "2023-09-26" @default.
- W2085829690 title "Preparation and Structure of Rhenium Fluoride Trioxide ReO3F, and the Polymorphism of Rhenium Trifluoride Dioxide, ReO2F3." @default.
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- W2085829690 doi "https://doi.org/10.1002/chin.200607007" @default.
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