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• W2085850863 abstract "The first gram-scale syntheses of two hyaluronan disaccharides are described. Construction of the (1 → 4)-linked disaccharide 12 was achieved in 12% overall yield using 2,3-bis-dimethyl acetal protection in combination with chlorosilane-induced carbamate cleavage methodologies. The uronic acid functionality was installed using TEMPO oxidation with NaOCl as the hypochlorite source. The (1 → 3)-linked disaccharide 18 was achieved in 7% overall yield utilizing acetonide protection in addition to the chlorosilane-induced carbamate cleavage methodology and the TEMPO oxidation." @default.
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• W2085850863 date "2004-05-01" @default.
• W2085850863 modified "2023-10-07" @default.
• W2085850863 title "Gram-scale syntheses of the (1 → 3)-linked and (1 → 4)-linked hyaluronan disaccharides" @default.
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• W2085850863 doi "https://doi.org/10.1016/j.carres.2004.03.005" @default.
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