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- W2086307907 abstract "In addition to the already known 3β,6α-dihydroxy-5α-pregn-9(11)-en-20-one (1), 3β,6α,20ξ-trihydroxy-5α-cholest-9(11)-en-23-one (2), 3β,6α,20ξ-trihydroxy-24ξ-methyl-5α-cholest-9(11)-en-23-one (3) [isolated in the form of the diacetates 1′, 2′, and 3′ from the enzymatic hydrolyzate of an oligoglycoside mixture], and thornasteroside A (8) a new genuine oligoglycoside sulfate named versicoside A has been isolated and structurally elucidated by chemical and spectroscopic evidences as the monosodium salt of 6α-[(O-β-D-galactopyranosyl-(1→3)-O-β-D-fucopyranosyl-(1→2)-O-β-D-galactopyranosyl-(1→4)-O-[β-D-quinovopyranosyl-(1→2)]-O-β-D-xylopyranosyl-(1→3)-β-D-quinovopyranosyl)oxy]-20ξ-hydroxy-3β-(sulfooxy)-5α-cholest-9(11)-en-23-one (4). Biologisch aktive Glycoside aus Asteroidea, V. - Steroid-Oligoglycoside aus dem Seestern Asterias amurensis [cf.] versicolor Sladen, 1. - Strukturermittlung eines neuen Oligoglycosidsulfats Neben den bereits bekannten Steroiden 3β,6α-Dihydroxy-5α-pregn-9(11)-en-20-on (1), 3β,6α,20ξ-Trihydroxy-5α-cholest-9(11)-en-23-on (2), 3β,6α,20ξ-Trihydroxy-24ξ-methyl-5α-cholest-9(11)-en-23-on (3) [isoliert in Form ihrer Acetate 1′, 2′ und 3′ aus dem enzymatischen Hydrolysat des Oligoglycosidgemischs] und Thornasterosid A (8) wurde ein neues, mit Versicosid A bezeichnetes genuines Oligoglycosidsulfat isoliert und dessen Struktur auf Grund chemischer und spektroskopischer Befunde als Mononatriumsalz von 6α-[(O-β-D-galactopyranosyl-(1→3)-O-β-D-fucopyranosyl-(1→2)-O-β-D-galactopyranosyl-(1→4)-O-[β-D-chinovopyranosyl-(1→2)]-O-β-D-xylopyranosyl-(1→3)-β-D-chinovopyranosyl)oxy]-20ξ-hydroxy-3β-(sulfooxy)-5α-cholest-9(11)-en-23-on (4) ermittelt." @default.
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- W2086307907 date "1983-12-15" @default.
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- W2086307907 title "Biologically Active Glycosides from Asteroidea, V. Steroid Oligoglycosides from the StarfishAsterias amurensis [cf.]versicolor Sladen, 1 Structural Elucidation of a New Oligoglycoside Sulfate" @default.
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