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- W2086379140 abstract "A new quantitative technique for determination of hydrogen in steels has been developed using levitation, which permits flotation and melting of samples by magnetic pressure under application of a high-frequency magnetic field to steel specimens. Steel samples are melted in a state of levitation in a flow of nitrogen gas. The discharged hydrogen gas is detected and measured quantitatively with a thermal conductivity detector. This method needs no crucible because the melting occurs in flotation. A cylindrical-shaped steel sample of 6 mm diameter and 6 mm length (about 1.5 g) was melted using the levitation melting technique. Radio frequency power of 1.5 kW with 200 kHz was applied to the levitation coil. Hydrogen was completely extracted within 1 min after melting. Working reference materials of stainless steel samples were analyzed in order to evaluate the present analytical method. The calibration curve showed an excellent linearity in a range of 0.4−6.7 μg/g, with a relative standard deviation of about 13% at the 1 μg/g level." @default.
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- W2086379140 date "1996-01-01" @default.
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- W2086379140 title "Determination of Hydrogen in Steel by Using a Levitation Melting Method" @default.
- W2086379140 doi "https://doi.org/10.1021/ac960377g" @default.
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