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- W2086514863 abstract "Abstract By DSC, X-ray diffraction and neutron powder diffraction the temperature behaviour of the K 1− x Rb x AlF 4 compounds is investigated in the concentration range x = 0 to x = 0.10. For large crystals it is shown that if x is greater than 0.02 the shear transformation of pure KAlF 4 splits into two structural phase transitions. The structures are determined by neutron powder profile refinement and the space groups P 4/ mbm , P 2 1 and P 2 1 / m are attributed to the three successive phases. The high and low temperature phases are the same as in pure KAlF 4 . The intermediate phase is derived from the T1AlF 4 type structure by AlF 6 octahedra rotations corresponding to the a 1 p b + p c + tilts system. It is shown that the temperature of the transition leading to the low temperature phase is sample size dependent." @default.
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- W2086514863 date "1987-03-01" @default.
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- W2086514863 title "Temperature behaviour of the tetrafluoroaluminates K1−xRbxAlF4. Evolution of the shear structural phase transition" @default.
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- W2086514863 doi "https://doi.org/10.1016/0038-1098(87)90164-5" @default.
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