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- W2086620152 abstract "Thin crystals of Zr4ON3F5 were investigated by high-resolution electron microscopy and holography in order to proof the value of electron holography to the investigation of complicated structures. The images reveal specific modulations of the basic fluorite structure and it was interesting what kind of information about the structure can be received from conventional imaging and from holography. The contrast of the high-resolution image in the ordered part of the crystal can be interpreted and calculated from a fluorite-related superstructure with the b-axis four times that of fluorite. A second modulation of the structure along its c-axis, caused by a reaction under observation conditions in the electron microscope and obvious not so regular like the modulation from the superstructure, could not be explained from high-resolution images. This led us to record an electron hologram of such a region of the crystal and to investigate the structure using techniques strongly related to electron holography. The image reconstruction from a high-resolution electron hologram, using Fourier filtering to select only the fluorite beams, suggests that this second modulation is due to dislocations in the metal lattice, which create stacking faults in the structure." @default.
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- W2086620152 date "1994-01-01" @default.
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- W2086620152 title "Combination of high-resolution electron imaging and holography in the investigation of the modulated structure of Zr4ON3F5" @default.
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- W2086620152 doi "https://doi.org/10.1016/0304-3991(94)90104-x" @default.
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