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- W2086653109 abstract "The 2,2,6,6-tetramethyl-1-piperidinyloxy free radical (TEMPO) mediated electrochemical oxidation of d-glucose to d-glucaric acid on a synthetically useful scale is reported. Using TEMPO and a graphite felt anode combined with a stainless steel cathode, d-glucose was oxidized under different conditions (pH, temperature, co-oxidant), and the reaction outcomes were analyzed. Optimized conditions for such oxidation are provided along with few new interesting results unique to this reaction, such as the appearance of a novel triacid." @default.
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- W2086653109 date "2010-04-01" @default.
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- W2086653109 title "Improved preparative electrochemical oxidation of d-glucose to d-glucaric acid" @default.
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- W2086653109 doi "https://doi.org/10.1016/j.electacta.2009.11.041" @default.
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