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• W2086690136 abstract "(-)-Indolactam-V (IL-V) (1) -was prepared in 10 steps from L-tryptophan methyl ester in 17.1% overall yield. The key steps involve regiospecific thallation of the acylindole intermediate (4), followed by azide displacement and reduction to introduce the 13-amino group. Control of the C-ll stereocenter was achieved by SN2 displacement of the chiral inflate (10), derived from D-valine. The thallium mediated closure of dipeptide (17) did not provide an alternative route to IL-V." @default.
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• W2086690136 date "1990-01-01" @default.
• W2086690136 modified "2023-09-25" @default.
• W2086690136 title "A Regio- and stereocontrolled total synthesis of (-)-indolactam-V" @default.
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• W2086690136 doi "https://doi.org/10.1016/s0040-4020(01)87853-4" @default.
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