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• W2086933486 abstract "The crystalline structure of a 7Li and 11B labeled lithium borohydride has been investigated using neutron powder diffraction at 3.5, 360, and 400 K. The B–H bond lengths and H–B–H angles for the [BH4]− tetrahedra indicated that the tetrahedra maintained a nearly ideal configuration throughout the temperature range investigated. The atomic displacement parameters at 360 K suggest that the [BH4]− tetrahedra become increasingly disordered as a result of large amplitude librational and reorientational motions as the orthorhombic to hexagonal phase transition (T=384 K) is approached. In the high-temperature hexagonal phase, the [BH4]− tetrahedra displayed extreme disorder about the trigonal axis along which they are aligned. Neutron vibrational spectroscopy data were collected at 5 K over an energy range of 10–170 meV, and were found to be in good agreement with prior Raman and low-resolution neutron spectroscopy studies." @default.
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• W2086933486 date "2007-04-01" @default.
• W2086933486 modified "2023-10-13" @default.
• W2086933486 title "Structure and vibrational dynamics of isotopically labeled lithium borohydride using neutron diffraction and spectroscopy" @default.
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• W2086933486 doi "https://doi.org/10.1016/j.jssc.2007.01.031" @default.
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