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- W2087130296 abstract "A simple, efficient and high-yielding process has been developed for the synthesis of unprecedented symmetrical trans-α,α′-bis(diphenylphosphoryl)cycloalkanols (2a-d), through the p-toluenesulfonic acid-catalyzed reduction of trans-α,α′-bis(diphenylphosphoryl)cycloalkanones with sodium borohydride in ethanol at room temperature. The structures of the synthesized compounds were studied using various spectroscopic tools including IR, NMR (1H, 31P, 13C) spectroscopy and mass spectrometry. The molecular structure of compound (2a) was further investigated using single crystal X-ray diffraction analysis. The Hirshfeld surface, curvedness, shape index and 2D-fingerprint plots were used to evaluate various intermolecular interactions within the crystal structure. UV-Vis and HOMO-LUMO properties of compound (2a) were also investigated." @default.
- W2087130296 created "2016-06-24" @default.
- W2087130296 creator A5061926426 @default.
- W2087130296 creator A5088061181 @default.
- W2087130296 date "1982-12-01" @default.
- W2087130296 modified "2023-09-25" @default.
- W2087130296 title "Solvent extraction properties of ditertiaryphosphine dioxides" @default.
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- W2087130296 doi "https://doi.org/10.1016/0010-8545(82)85035-2" @default.
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