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W2087185887 abstract "Abstract A solution of C 60 in toluene reacts with Pd(dba) 2 or Pd 2 (dba) 3 (dba = dibenzylideneacetone) and monophosphanes in a 1:1:2 molar ratio to give the corresponding Pd monophosphane fullerene derivatives [Pd(η 2 ‐C 60 )L 2 ] [L = P(2‐Fu) 3 (Fu = furyl) 1 ; L = P(2‐Fu)Ph 2 2 ; L = PPh 2 H 3 ; L = P(Fc)Ph 2 (Fc = ferrocenyl) 4 ; L = P(Fc) 2 Ph 5 ], whereas reaction with M(dba) 2 (M = Pd, Pt) and subsequent treatment with diphosphanes in 1:1:1 molar ratio afforded the corresponding Pd/Pt diphosphane fullerene complexes [Pd(η 2 ‐C 60 ){Ph 2 PCH 2 (CH 2 OCH 2 ) n CH 2 PPh 2 }] ( n = 1 6 ; n = 2 7 ; n = 3 8 ) and [Pt(η 2 ‐C 60 ){Ph 2 PCH 2 (CH 2 OCH 2 ) n CH 2 PPh 2 }] ( n = 1 9 ; n = 2 10 ; n =3 11 ). All the new fullerene complexes 1 − 11 were characterized by elemental analysis, IR, 1 H NMR and 31 P NMR spectroscopy, as well as by X‐ray diffraction analysis (for 7 ). The optical limiting properties of 3 − 5 were determined and the possible pathways for the “one pot” reactions leading to 1 − 11 are briefly discussed. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2004)" @default.
W2087185887 created "2016-06-24" @default.
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W2087185887 date "2004-02-01" @default.
W2087185887 modified "2023-09-23" @default.
W2087185887 title "Synthesis, Characterization and Properties of Transition Metal Pd/Pt [60]Fullerene Complexes Containing Phosphane Ligands − Crystal Structure of [Pd(η 2 ‐C 60 ){Ph 2 PCH 2 (CH 2 OCH 2 ) 2 CH 2 PPh 2 }]" @default.
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W2087185887 doi "https://doi.org/10.1002/ejic.200300513" @default.
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