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- W2087209213 abstract "Abstract We have synthesised a diazonium ion starting from 2-chloro-5-aminobenzyl alcohol, and investigated in detail its thermal stability. The DSC runs at seven different heating rates give evidence of a single decomposition reaction occurring around 90–120 °C, whose kinetics were analysed by both the iso-conversional differential and integral method, the invariant kinetic parameters method, Kissinger's method, and a differential isothermal method. All of these methods led to similar values for the kinetic parameters and showed that the first-order mechanism fits the data best. The values of the kinetic parameters were further used for calculating the half-life time of the ion at various temperatures. The result of the stability prediction at 60 °C was compared with that of an analytical isothermal test yielding a good agreement between prediction and experiment." @default.
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- W2087209213 date "2002-01-01" @default.
- W2087209213 modified "2023-09-27" @default.
- W2087209213 title "Investigations on the thermal stability of a diazonium ion on solid support" @default.
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- W2087209213 doi "https://doi.org/10.1016/s0141-3910(01)00235-x" @default.
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