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- W2087422833 abstract "Total spectral assignment of the bis-indole alkaloid Navelbine®, 5′-nor-anhydrovinbIastine, was accomplished using a combination of two-dimensional nmr techniques. Conventional homonuclear and inverse-detected experiments were supplemented with the HMQC-TOCSY experiment to unequivocally assign carbons directly bound to overlapped protons. In addition, the recently introduced GEM-COSY experiment was evaluated as a technique for the identification of geminal methylene pairs. Partial assignments proposed by Potier and co-workers, based on chemical shift considerations, are largely in agreement with the unequivocal assignments determined in this study." @default.
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- W2087422833 date "1992-01-01" @default.
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- W2087422833 title "Total assignment of the proton and carbon NMR spectra of 5′-NOR-anhydrovinblastine" @default.
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- W2087422833 doi "https://doi.org/10.1002/jhet.5570290151" @default.
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