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- W2087443407 abstract "The low temperature 1H NMR spectra in d-chloroform of the ternary complexes bis-(8-quinolinato) tin(IV) dichloride, bis-(5,7 dichloro-8-quinolinato) tin(IV) dichloride, and bis-(2 methyl-5,7-dichloro-8-quinolinato) tin(IV) dichloride have been obtained. The spectra showed that for the three complexes, only two configurations were appreciably populated, their free energy differences being equal to 0.28, 0.08 and −0.04 kcal/mol respectively. The proton chemical shifts, the 1H-1H coupling constants and some of the 1H-119Sn coupling constants have been obtained for each complex in the two configurations. An approximate computation of chemical shifts, including aromatic ring magnetic anisotropies and electric effects from polar groups, allowed the identification of the two configurations as the cis-cis-trans and the cis-trans-cis (with respect to Cl, N and O atoms), the former being the more populated one." @default.
- W2087443407 created "2016-06-24" @default.
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- W2087443407 date "1983-01-01" @default.
- W2087443407 modified "2023-10-14" @default.
- W2087443407 title "Proton NMR spectra and structure of chlorotin(IV) ternary complexes of 8-quinolinol and its 5,7 dichloro and 2 methyl-5,7 dichloro derivatives" @default.
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- W2087443407 doi "https://doi.org/10.1016/s0277-5387(00)81442-4" @default.
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