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- W2087612773 abstract "The conversion of (±)-hydratropaoyl chloride into (S)-(+)-hydratropic acid (4) can be achieved with (S)-(−)-1-phenylethanol (2) as chiral auxiliary agent in the following way: Generation of the ketene (1) from the acid chloride in situ, reaction with (S)-(−)-(2) in the presence of a base to give a mixture of the diastereomers (3) [with pyridine, e.g., (S,S) :(R,S) = 88 :12], hydrolysis of (S)-(+)-(4) with recovery of (S)-(−)-(2)." @default.
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- W2087612773 date "1981-10-01" @default.
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- W2087612773 title "Base Catalyzed Asymmetric Induction of the Reaction of Methyl(phenyl)ketene with 1-Phenylethanol: Method of Obtaining Hydratropic Acid in High Enantiomeric Purity" @default.
- W2087612773 doi "https://doi.org/10.1002/anie.198108852" @default.
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