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• W2087666075 abstract "A measurement-based closed-loop control system using in-process ATR-FTIR spectroscopy coupled with a multivariate chemometric PLS calibration model is developed, validated, and applied to the monitoring and control of supersaturation in a 250- L industrial pilot-plant crystalliser. Supersaturation control experiments are carried out on seeded batch cooling crystallisation of β-l-glutamic acid from aqueous solutions using two methods of seeding involving addition of seeds to the solution and generation of seeds within the solution. The generic applicability of the approach is demonstrated through this challenging system reflecting this molecule’s weak chromophore for infrared and relatively low solubility compared with previous solute−solvent systems. Based on the laboratory experiments, the system was fully tested and optimised prior to a series of trials carried out in an industrial pilot plant at Syngenta, Munchwillen, Switzerland. Good control of the supersaturation is achieved at three levels, 1.1, 1...." @default.
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• W2087666075 date "2011-03-14" @default.
• W2087666075 modified "2023-09-23" @default.
• W2087666075 title "In-Process Monitoring and Control of Supersaturation in Seeded Batch Cooling Crystallisation of l-Glutamic Acid: From Laboratory to Industrial Pilot Plant" @default.
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• W2087666075 doi "https://doi.org/10.1021/op100223a" @default.
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