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• W2087839780 abstract "The severe depolymerisation that occurs when cellulose is oxidised by periodate can be greatly diminished by carrying out the oxidation in steps, with borohydride reduction after each, and by using propan-1-ol as a radical scavenger in the oxidation steps. The reduction steps greatly increase the rate of Malapradian oxidation by eliminating hemiacetal structures and increasing the solubility of the substrate. They also minimise free-radical-mediated depolymerisation, and prevent the over-oxidation (stepwise peeling) that otherwise ensues at the newly liberated reducing end-groups. The use of regenerated cellulose or mercerised cellulose in order to increase accessibility is also advantageous. Depolymerisation by β-elimination in the reduction steps can be minimised by using very concentrated aqueous sodium borohydride. By these methods, a sample of fully oxidised and reduced cellulose with Mn = 132,000 was prepared." @default.
• W2087839780 created "2016-06-24" @default.
• W2087839780 creator A5082002287 @default.
• W2087839780 date "1988-08-01" @default.
• W2087839780 modified "2023-09-24" @default.
• W2087839780 title "Control of depolymerisation during the preparation of reduced dialdehyde cellulose" @default.
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• W2087839780 doi "https://doi.org/10.1016/0008-6215(88)84123-5" @default.
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