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• W2087995503 abstract "Recoverable BINAM-prolinamide derivatives, as well as l-proline, give results complementary to antibodies when used as organocatalysts for aldol reactions between aldehydes and α-alkoxyacetones driving regioselectively to anti/syn-1,2-diols. The formation of the iso-regioisomer is suppressed using α-hydroxyacetone in DMSO at rt, achieving the corresponding anti-1,2-diol with ee’s up to 85%. For α-alkoxyacetones (methoxy, benzyloxy, and tert-butyldimethylsilyloxy), the highest regio- and diastereoselectivity is achieved using α-methoxyacetone in DMF at 0 °C; the enantiomeric excess for the anti-1,2-isomer being up to 98%." @default.
• W2087995503 created "2016-06-24" @default.
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• W2087995503 date "2006-04-01" @default.
• W2087995503 modified "2023-10-03" @default.
• W2087995503 title "Organocatalyzed direct aldol condensation using l-proline and BINAM-prolinamides: regio-, diastereo-, and enantioselective controlled synthesis of 1,2-diols" @default.
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• W2087995503 doi "https://doi.org/10.1016/j.tetasy.2006.03.023" @default.
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