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• W2088082685 abstract "A new catalyst for the copolymerization of ethylene and α-olefins, based on (η5-C5Me5)TiCl3, methanol, 2,6-di-t-butylphenol, and methylaluminoxane, is described. The polymerization behavior indicates the necessity of the hindered phenol for high activity, but does not prove that a phenoxide group exists in the coordination sphere of the active site. The titanium K-edge EXAFS spectra of mixtures of various combinations of the four components are best fit to a structure containing a short TiO bond, a Ti–arene interaction, and two alkyl carbons. XANES, and to a lesser extent X-ray photoelectron spectroscopy (XPS), spectra show that the presence of the alcohol(s) in the catalyst is correlated with higher titanium absorption energies as well as narrower peak widths." @default.
• W2088082685 created "2016-06-24" @default.
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• W2088082685 date "2001-07-01" @default.
• W2088082685 modified "2023-09-25" @default.
• W2088082685 title "Synchrotron XAS studies on a half-sandwich titanium-based polyethylene catalyst" @default.
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• W2088082685 doi "https://doi.org/10.1016/s1381-1169(01)00126-1" @default.
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