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• W2088239962 startingPage "7094" @default.
• W2088239962 abstract "Ir(I)-catalyzed intermolecular allylic amidation of ethyl allylic carbonates with soft nitrogen nucleophiles under completely salt-free conditions is described. A combination of [Ir(COD)Cl](2), a chiral phosphoramidite ligand L*, and DBU as a base in THF effects the reaction. The reaction appears to be quite general, accommodating a wide variety of R-groups and soft nitrogen nucleophiles, and proceeds with excellent regio- and enantioselectivities to afford the branched N-protected allylic amines. The developed reaction was conveniently utilized in the asymmetric synthesis of Boc protected alpha- and beta-amino acids as well as (-)-cytoxazone." @default.
• W2088239962 created "2016-06-24" @default.
• W2088239962 creator A5029618034 @default.
• W2088239962 creator A5035086279 @default.
• W2088239962 date "2007-10-01" @default.
• W2088239962 modified "2023-10-18" @default.
• W2088239962 title "Iridium(I)-catalyzed regio- and enantioselective allylic amidation" @default.
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• W2088239962 doi "https://doi.org/10.1016/j.tetlet.2007.08.009" @default.
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