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• W2088596952 abstract "A double-quantum homonuclear correlation nuclear magnetic resonance experiment for dipolar-coupled half-integer quadrupolar nuclei in solids is presented. The experiment is based on rotary resonance dipolar recoupling and uses bracketed spin-lock pulses to excite double-quantum coherence and later to convert it to the zero-quantum one. A central-transition-selective π pulse at the beginning of the t1 evolution period differentiates coherence transfer pathways of double-quantum coherences arising from coupled spins and from a single spin, so that the latter can be efficiently filtered out by phase cycling. The experiment was tested on an aluminophosphate molecular sieve AlPO4-14, a material with a variety of aluminum quadrupolar coupling constants, isotropic chemical shifts and homonuclear distances. In a two-dimensional spectrum aluminum dipolar couplings with internuclear distances between 2.9 and 5.5 Å were resolved. Although the experiment requires an application of weak radio-frequency fields, frequency offsets did not affect its performance crucially." @default.
• W2088596952 created "2016-06-24" @default.
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• W2088596952 date "2004-02-08" @default.
• W2088596952 modified "2023-10-17" @default.
• W2088596952 title "Double-quantum homonuclear correlation magic angle sample spinning nuclear magnetic resonance spectroscopy of dipolar-coupled quadrupolar nuclei" @default.
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• W2088596952 doi "https://doi.org/10.1063/1.1638741" @default.
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