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- W2088753783 abstract "A method for the simultaneous analysis of pipecolic acid and proline in the brain is developed. The qualification and quantification of pipecolic acid and proline are accomplished with gas chromatography/mass spectrometry including a selected ion-monitoring technique by using deuterium-labeled proline as an internal standard, after the amino and carboxylic groups of these cyclic amino acids are derivatized with boron trifluoride methanol complex and heptafluorobutyric anhydride. The lower limit of quantification for the method is picomole levels and the concentration of pipecolic acid and proline in rat whole brain is determined to be 1.05 and 71.50 nmol/g of tissue, respectively." @default.
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- W2088753783 date "1981-10-01" @default.
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- W2088753783 title "Simultaneous analysis of pipecolic acid with proline in the brain by selected ion-monitoring technique" @default.
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- W2088753783 doi "https://doi.org/10.1016/0003-2697(81)90710-7" @default.
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