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• W2088771845 endingPage "5064" @default.
• W2088771845 startingPage "5057" @default.
• W2088771845 abstract "Multiwalled carbon nanotubes (MWNTs) (diameter range, 10−20 nm) were functionalized with 4-methoxybenzoic acid and 4-ethoxybenzoic acid via a Friedel−Crafts reaction in polyphosphoric acid to afford methoxybenzoyl- and ethoxybenzoyl-functionalized MWNTs. As-received MWNT, methoxybenzoyl-functionalized (MeO-MWNT), and ethoxybenzoyl-functionalized (EtO-MWNT) nanotubes were dispersed in ethylene glycol (EG). Because of the structural similarity, the mixture of EtO-MWNT (0.4 wt %) and EG was a homogeneous dispersion, whereas MeO-MWNT and pristine MWNT were dispersed in EG rather heterogeneously at the same loading. In situ polycondensation of EG and terephthalic acid in the presence of pristine MWNT, MeO-MWNT, or EtO-MWNT was carried out to generate the corresponding MWNT/PET, MeO-MWNT/PET, and EtO-MWNT/PET nanocomposites. High molecular weight poly(ethylene terephthalates) (PETs), with intrinsic viscosity range 0.6−0.7 dL/g (o-chlorophenol at 30 ± 0.1 °C), were obtained in all cases. In comparing the images from scanning electron microscopy (SEM) taken at the same magnification for these nanocomposites, it is clear that the MWNT/PET system has poor MWNT dispersion and the MeO-MWNT/PET system has a better dispersion. However, EtO-MWNT in PET matrix is most homogeneously dispersed, and the interfacial boundary between EtO-MWNT and PET matrix is practically nondiscernible." @default.
• W2088771845 created "2016-06-24" @default.
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• W2088771845 date "2005-09-03" @default.
• W2088771845 modified "2023-10-16" @default.
• W2088771845 title "<i>In Situ</i> Synthesis of Poly(ethylene terephthalate) (PET) in Ethylene Glycol Containing Terephthalic Acid and Functionalized Multiwalled Carbon Nanotubes (MWNTs) as an Approach to MWNT/PET Nanocomposites" @default.
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• W2088771845 doi "https://doi.org/10.1021/cm051218t" @default.
• W2088771845 hasPublicationYear "2005" @default.
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