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- W2088897500 abstract "A thermo-responsive and macroporous monolithic cryogel was directly prepared by in situ free-radical redox cryo-polymerization in a stainless steel chromatographic column (100 mm × 4.6mm i.d.) using N-isopropylacrylamide (NIPAAm) as functional monomer and PEG-20,000 as porogen at -12°C. The internal morphology of resulting monolithic cryogel was estimated by scanning electron microscopy (SEM). Based on that, a submicron skeleton structure was observed. Besides, the gravimetrically determined rates of swelling/deswelling for thermo-responsive monolithic cryogel were much higher than that of hydrogel adopting the same component proportion via conventional method (25°C for 24h). Simultaneously, a temperature-dependent resolution of steroids was also achieved using only water as a mobile phase. The theoretical plate number of every analyte was more than 2000." @default.
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- W2088897500 date "2011-08-01" @default.
- W2088897500 modified "2023-09-26" @default.
- W2088897500 title "Investigation of temperature-responsivity and aqueous chromatographic characteristics of a thermo-responsive monolithic column" @default.
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- W2088897500 doi "https://doi.org/10.1016/j.talanta.2011.05.034" @default.
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