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• W2089241657 abstract "The 1H and 13C NMR spectra of D-amygdalin, a cyanogenetic disaccharide accumulated in food plants, were assigned using a combination of NMR techniques. Methods applied include standard 1H–1H COSY, proton zero quantum coherence (ZQCOSY), 1D NOE, broad-band decoupled 1H–13C chemical shift correlation and long-range 1H–13C chemical shift correlation. ZQCOSY was especially useful in assigning the closely spaced sugar resonances, and long-range 1H-13C chemical shift correlation allowed sequencing of the monosaccharide rings. Coupling constants useful in conformational analysis are derived from highly digitized 1H 1D spectra and 2D J-resolved spectroscopy. The 1H and 13C chemical shifts and coupling constants indicate that the β-D-glucopyranose rings of D-amygdalin adopt a 4C1 chair conformation." @default.
• W2089241657 created "2016-06-24" @default.
• W2089241657 creator A5011164163 @default.
• W2089241657 date "1990-09-01" @default.
• W2089241657 modified "2023-09-27" @default.
• W2089241657 title "1H and13C NMR analysis ofD-amygdalin: Oligosaccharide assignment and sequencing" @default.
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• W2089241657 doi "https://doi.org/10.1002/mrc.1260280907" @default.
• W2089241657 hasPublicationYear "1990" @default.
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