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• W2089601744 abstract "Ethylenethiourea (ETU) is a major metabolite of ethylenebisdithiocarbamate pesticides: a sensitive and specific assay for its determination in human urine is proposed below. ETU is extracted on a diatomaceous earth column using dichloromethane and derivatized with the mixture of N-(tert-butyldimethylsilyl)-N-methyltrifluoroacetamide and tert-butyldimethyilsilyl chloride. The derivative is analyzed using GC/MS in the EI/SIM mode. The whole procedure is carried out in the presence of ethylenethiourea-d4 as internal standard. The analytical features of the method are: high specificity, >90% recovery, range of linearity 0–200 μg/L, within- and between-run precision as coefficient of variation, <17 and <20%, respectively, limit of quantification 2 μg/L. In specimens stored in the dark at −20 °C ETU is stable for at least 6 months. The procedure was successfully applied to the biological monitoring of vineyard workers exposed to EBDTC and of a matched group of subjects from the general population." @default.
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• W2089601744 date "2005-01-25" @default.
• W2089601744 modified "2023-10-17" @default.
• W2089601744 title "Application of gas chromatography-mass spectrometry for the determination of urinary ethylenethiourea in humans" @default.
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• W2089601744 doi "https://doi.org/10.1016/j.jchromb.2004.10.042" @default.
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