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• W2089773502 startingPage "1625" @default.
• W2089773502 abstract "We report a facile synthetic approach of high-quality chromium(III) terephthalate [MIL-101(Cr)] by acetate-assisted method in the absence of toxic HF. Results indicate that the morphology and surface area of the MIL-101(Cr) can be tuned by modifying the molar ratio of acetate/<TEX>$Cr(NO_3)_3$</TEX>. The Brunauer-Emmett-Teller (BET) surface area of MIL-101(Cr) synthesized at the optimized condition can exceed 3300 <TEX>$m^2/g$</TEX>. It is confirmed that acetate could promote the dissolution of di-carboxylic linker and accelerate the nucleation ratio. So the pure and small size of MIL-101(Cr) with clean pores can be obtained. <TEX>$CO_2$</TEX>, <TEX>$CH_4$</TEX> and <TEX>$N_2$</TEX> adsorption isotherms of the samples are studied at 298 K and 313 K. Compared with the traditional method, MIL-101(Cr) synthesized by acetate-assisted method possess enhanced <TEX>$CO_2$</TEX> selective adsorption capacity. At 1.0 bar 298 K, it exhibits 47% enhanced <TEX>$CO_2$</TEX> adsorption capacity. This may be attributed to the high surface area together with clean pores of MIL-101(Cr)." @default.
• W2089773502 created "2016-06-24" @default.
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• W2089773502 date "2013-06-20" @default.
• W2089773502 modified "2023-10-07" @default.
• W2089773502 title "Acetate-assisted Synthesis of Chromium(III) Terephthalate and Its Gas Adsorption Properties" @default.
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• W2089773502 doi "https://doi.org/10.5012/bkcs.2013.34.6.1625" @default.
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