FRINK Linked Data Fragments server

Matches in SemOpenAlex for { <https://semopenalex.org/work/W2089868110> ?p ?o ?g. }

• W2089868110 endingPage "907" @default.
• W2089868110 startingPage "901" @default.
• W2089868110 abstract "Pharmaceuticals residues in the environment have become a growing scientific interest worldwide. In the light of the possible harmful effects of tobramycin, a rapid and sensitive analytical method for determination of tobramycin in soil was developed. The extraction and purification methods, derivatization conditions, and chromatographic conditions in the determination of tobramycin in soil have been fully investigated. Extraction was carried out by a combination of vortex mixer and ultrasonic oscillation using acetone/water as the extraction agent. The extract was concentrated to 1 mL and passed through the C18 SPE cartridge rinsed with water (3 mL), methanol (3 mL). The derivatization procedure was followed by the reaction of tobramycin with 4-Chloro-3,5-dinitrobenzotrifluoride at 60 °C for 10 min in pH 9.0 H3BO3–Na2B4O7 medium. The labeled tobramycin was determined by high performance liquid chromatography at 245 nm. Separation was accomplished within 15 min in gradient elution mode with trifluoroacetic acid in mobile phase as ion-pair reagent. The correlation coefficient for the method was 0.9999 in concentrations ranging from 0.10 to 100.0 μg/g. The limit of detection was 0.02 μg/g for tobramycin in soil at a signal-to-noise ratio of 3. The calculated recoveries of the proposed method were from 78.0 to 91.0% and RSDs were 3.38–9.79% in the application to the quantitative determination of tobramycin in all types of soil. The method will help to establish adequate monitoring of tobramycin residue in soil and make the contribution to environmental behavior evaluation." @default.
• W2089868110 created "2016-06-24" @default.
• W2089868110 creator A5005227426 @default.
• W2089868110 creator A5042322241 @default.
• W2089868110 creator A5047767249 @default.
• W2089868110 creator A5049728886 @default.
• W2089868110 creator A5069030526 @default.
• W2089868110 creator A5078446885 @default.
• W2089868110 creator A5079477143 @default.
• W2089868110 date "2011-04-01" @default.
• W2089868110 modified "2023-10-17" @default.
• W2089868110 title "Determination of tobramycin in soil by HPLC with ultrasonic-assisted extraction and solid-phase extraction" @default.
• W2089868110 cites W1973201731 @default.
• W2089868110 cites W1991266217 @default.
• W2089868110 cites W1999126484 @default.
• W2089868110 cites W2021388902 @default.
• W2089868110 cites W2022957538 @default.
• W2089868110 cites W2027302919 @default.
• W2089868110 cites W2034596339 @default.
• W2089868110 cites W2035376565 @default.
• W2089868110 cites W2043539809 @default.
• W2089868110 cites W2044673195 @default.
• W2089868110 cites W2053442312 @default.
• W2089868110 cites W2054721976 @default.
• W2089868110 cites W2055244789 @default.
• W2089868110 cites W2056432919 @default.
• W2089868110 cites W2057857501 @default.
• W2089868110 cites W2066264157 @default.
• W2089868110 cites W2070817339 @default.
• W2089868110 cites W2071887537 @default.
• W2089868110 cites W2073289588 @default.
• W2089868110 cites W2073351220 @default.
• W2089868110 cites W2081502298 @default.
• W2089868110 cites W2084507393 @default.
• W2089868110 cites W2087319972 @default.
• W2089868110 cites W2089618866 @default.
• W2089868110 cites W2092717176 @default.
• W2089868110 cites W2119566321 @default.
• W2089868110 cites W2128387115 @default.
• W2089868110 cites W2155435049 @default.
• W2089868110 cites W2159570378 @default.
• W2089868110 cites W2164562908 @default.
• W2089868110 cites W2313392321 @default.
• W2089868110 cites W2326895856 @default.
• W2089868110 cites W2913098477 @default.
• W2089868110 cites W73898233 @default.
• W2089868110 doi "https://doi.org/10.1016/j.jchromb.2011.02.042" @default.
• W2089868110 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/21429824" @default.
• W2089868110 hasPublicationYear "2011" @default.
• W2089868110 type Work @default.
• W2089868110 sameAs 2089868110 @default.
• W2089868110 citedByCount "19" @default.
• W2089868110 countsByYear W20898681102012 @default.
• W2089868110 countsByYear W20898681102013 @default.
• W2089868110 countsByYear W20898681102014 @default.
• W2089868110 countsByYear W20898681102015 @default.
• W2089868110 countsByYear W20898681102018 @default.
• W2089868110 countsByYear W20898681102019 @default.
• W2089868110 countsByYear W20898681102022 @default.
• W2089868110 countsByYear W20898681102023 @default.
• W2089868110 crossrefType "journal-article" @default.
• W2089868110 hasAuthorship W2089868110A5005227426 @default.
• W2089868110 hasAuthorship W2089868110A5042322241 @default.
• W2089868110 hasAuthorship W2089868110A5047767249 @default.
• W2089868110 hasAuthorship W2089868110A5049728886 @default.
• W2089868110 hasAuthorship W2089868110A5069030526 @default.
• W2089868110 hasAuthorship W2089868110A5078446885 @default.
• W2089868110 hasAuthorship W2089868110A5079477143 @default.
• W2089868110 hasConcept C119128265 @default.
• W2089868110 hasConcept C147789679 @default.
• W2089868110 hasConcept C179998833 @default.
• W2089868110 hasConcept C185592680 @default.
• W2089868110 hasConcept C2775832221 @default.
• W2089868110 hasConcept C2776923573 @default.
• W2089868110 hasConcept C2778974779 @default.
• W2089868110 hasConcept C2781338088 @default.
• W2089868110 hasConcept C40875361 @default.
• W2089868110 hasConcept C43617362 @default.
• W2089868110 hasConcept C4725764 @default.
• W2089868110 hasConcept C501593827 @default.
• W2089868110 hasConcept C55493867 @default.
• W2089868110 hasConcept C73826308 @default.
• W2089868110 hasConcept C81426234 @default.
• W2089868110 hasConceptScore W2089868110C119128265 @default.
• W2089868110 hasConceptScore W2089868110C147789679 @default.
• W2089868110 hasConceptScore W2089868110C179998833 @default.
• W2089868110 hasConceptScore W2089868110C185592680 @default.
• W2089868110 hasConceptScore W2089868110C2775832221 @default.
• W2089868110 hasConceptScore W2089868110C2776923573 @default.
• W2089868110 hasConceptScore W2089868110C2778974779 @default.
• W2089868110 hasConceptScore W2089868110C2781338088 @default.
• W2089868110 hasConceptScore W2089868110C40875361 @default.
• W2089868110 hasConceptScore W2089868110C43617362 @default.
• W2089868110 hasConceptScore W2089868110C4725764 @default.
• W2089868110 hasConceptScore W2089868110C501593827 @default.
• W2089868110 hasConceptScore W2089868110C55493867 @default.
• W2089868110 hasConceptScore W2089868110C73826308 @default.
• W2089868110 hasConceptScore W2089868110C81426234 @default.

• next