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- W2089899058 abstract "The alkylation of benzoic acid was studied in different solvents containing an alkyl halide and tetrabutylammonium bicarbonate. The bicarbonate anion was transferred to the organic solvents by shaking solid sodium bicarbonate with solutions of tetrabutylammonium hydrogen sulphate. The alkylation rate was influenced by the type of solvent used, ketones being the most favourable. The quaternary ammonium bicarbonate was found to be stable in the ketones even at elevated temperatures, but the dissolution was slower than in halogenated solvents. The possibility of controlling the alkylation reaction by a suitable choice of solvent, alkyl halide and reaction temperature was demonstrated. It was also shown that the content of water and ethanol in some solvents drastically affected the alkylation rate." @default.
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- W2089899058 date "1980-08-01" @default.
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- W2089899058 title "Alkylation of carboxylic acids by solid-liquid phase-transfer catalysis for determination by gas chromatography. II" @default.
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- W2089899058 doi "https://doi.org/10.1016/s0021-9673(00)80445-8" @default.
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