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- W2089989637 abstract "Iridium-catalyzed asymmetric allylic amination of allylic carbonates with 2-allylanilines was realized. With a catalyst generated from 2 mol% of [Ir(dbcot)Cl]2 (dbcot = dibenzo[a,e]cyclooctatetraene) and 4 mol% of phosphoramidite ligand (L3), the amination products were obtained in up to 99% yield and 99% ee. Subjecting amination products to trifluoroacetyl protection and ring-closing-metathesis reaction provided an efficient synthesis of enantioenriched 2,5-dihydrobenzo[b]azepine derivatives." @default.
- W2089989637 created "2016-06-24" @default.
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- W2089989637 date "2012-01-01" @default.
- W2089989637 modified "2023-09-26" @default.
- W2089989637 title "Enantioselective synthesis of 2,5-dihydrobenzo[b]azepine derivatives via iridium-catalyzed asymmetric allylic amination with 2-allylanilines and ring-closing-metathesis reaction" @default.
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- W2089989637 doi "https://doi.org/10.1039/c2ob00036a" @default.
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