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- W2090382530 endingPage "429" @default.
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- W2090382530 abstract "An efficient, economical, and convenient method was developed for the preparation of 2-substituted (N, O, C) benzothiazoles from N′-substituted-N-(2-halophenyl)thioureas, O′-substituted-N-(2-halophenyl) carbamothioates, or N-(2-halophenyl) thioamides via a base-promoted cyclization in dioxane without any transition metal. A one-pot variant combining the synthesis of the thiourea and the cyclization was also demonstrated. High yields were obtained, and a variety of functional groups were tolerated under these conditions. Transition-metal-free, mild reactive conditions, wide application scope, and shorter reaction times make this method superior to the reported methods for the synthesis of 2-substituted benzothiazoles and suitable for combinatorial format." @default.
- W2090382530 created "2016-06-24" @default.
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- W2090382530 date "2010-04-09" @default.
- W2090382530 modified "2023-09-25" @default.
- W2090382530 title "Metal-Free Synthesis of 2-Substituted (N, O, C) Benzothiazoles via an Intramolecular C−S Bond Formation" @default.
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- W2090382530 doi "https://doi.org/10.1021/cc9001839" @default.
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