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• W2090470946 abstract "The extremely stable microinterface between two immiscible electrolytic solutions (micro-ITIES) housed at the tip of a 25 μm diameter capillary, has given access to simple ion transfer of alkali metal ions for the first time at conventional supporting electrolyte concentrations (∼5 mM). This was made possible by a uniquely designed pipette holder that uses a syringe to back-fill the aqueous phase and also helps to adjust and maintain the ITIES at the capillary tip, which was continuously monitored using a CCD camera attached to a custom-designed microscope. The formal transfer potential, Δowϕiz+o′ for each of the ions (Li+, Na+, K+, Rb+ and Cs+) was determined by means of cyclic voltammetry along with differential pulse voltammetry. This thermodynamic constant is of great value as a point of reference for the quantitative evaluation of metal ion extraction through interfacial complexation at an ITIES. Since these ions typically limit the polarizable potential window, in the past Δowϕiz+o′ was estimated using the current–potential response at the edge of the voltammogram, a method developed through numerical calculations. Δowϕiz+o′ was also determined at a microhole ITIES, requiring minimal concentrations of the analyte and no supporting electrolyte." @default.
• W2090470946 created "2016-06-24" @default.
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• W2090470946 date "2012-09-01" @default.
• W2090470946 modified "2023-10-17" @default.
• W2090470946 title "Determination of alkali metal ion transfers at liquid|liquid interfaces stabilized by a micropipette" @default.
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• W2090470946 doi "https://doi.org/10.1016/j.jelechem.2012.08.013" @default.
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