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- W2090650098 abstract "ABSTRACT The microstructure of poly(1,3‐pentadiene) synthesized by cationic polymerization of 1,3‐pentadiene with t BuCl/TiCl 4 initiating system is analyzed using one‐dimensional‐ and two‐dimensional‐NMR spectroscopy. It is shown that unsaturated part of chain contains only homo and mixed dyads with trans −1,4‐, trans −1,2‐, and cis −1,2‐structures with regular and inverse (head‐to‐head or tail‐to‐tail) enchainment, whereas cis −1,4‐ and 3,4‐units are totally absent. The new quantitative method for the calculation of content of different structural units in poly(1,3‐pentadiene)s based on the comparison of methyl region of 13 C NMR spectra of original and hydrogenated polymer is proposed. The signals of tert ‐butyl head and chloromethyl end groups are identified in a structure of poly(1,3‐pentadiene) chain and the new approaches for the quantitative calculation of number‐average functionality at the α ‐ and ω ‐end are proposed. © 2013 Wiley Periodicals, Inc. J. Polym. Sci., Part A: Polym. Chem. 2013, 51, 3297–3307" @default.
- W2090650098 created "2016-06-24" @default.
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- W2090650098 date "2013-05-16" @default.
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- W2090650098 title "A new insight into the mechanism of 1,3‐dienes cationic polymerization. II. Structure of poly(1,3‐pentadiene) synthesized with <sup>t</sup>BuCl/TiCl<sub>4</sub> initiating system" @default.
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- W2090650098 doi "https://doi.org/10.1002/pola.26724" @default.
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