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- W2090771227 abstract "The chiral 1,1′-bis-acetals, bis-1,1′-[(2S, 4S)-(hydroxymethyl)-2-dioxane1,3]-ferrocene (3) and 1,1′-bis-1,1′-[(2S, 4S)-(methoxymethyl)-2-dioxane1,3]-ferrocene (4) were synthesized. (3) was crystallographically characterised. The ortholithiation of (4) was studied in various conditions. Fair yields of monosubstituted compounds could be obtained with a complete regioselectivity in favor of the 2 position but the diastereoselectivities were moderate (up to 35%). Some disubstituted compounds can be isolated but in low yields (up to 8%). The regioselectivity is complete in favor of the 2,2′-disubstituted isomer. Only the diastereoisomer with two opposite planar chiralities is observed." @default.
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- W2090771227 date "1998-08-01" @default.
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- W2090771227 title "Mono and difunctionalisation of chiral ferrocenyl bis-acetals. X-Ray crystal structure of bis-1,1′-[(2S, 4S)-(hydroxymethyl)-2-dioxane1,3]-ferrocene" @default.
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- W2090771227 doi "https://doi.org/10.1016/s0022-328x(98)00449-5" @default.
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