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- W2090831812 abstract "Validation of an analytical method for determining chloramphenicol residues in muscle tissue by gas chromatography–electron capture detection (GC-ECD) was performed according to the latest European Union criteria for the analysis of veterinary drugs in food, laid down by Commission Decision 2002/657/EC. The method using the meta isomer of chloramphenicol as an internal standard proved to be very selective, specific to other related phenicols and accurate to within +3.6% at a concentration level of 8.9 µg/kg, as present in the certified reference material available. The correlation coefficient of the calibration curve was 0.9991. At all three fortification levels studied (0.3, 0.45 and 0.6 µg/kg), repeatability and intra-laboratory reproducibility were <8 and ≤9%, respectively. The decision limit (CCα) and detection capability (CCβ) were 0.07 and 0.12 µg/kg, respectively. The validation results and the results of participation in an international inter-laboratory proficiency test indicate that the method presented is completely suited for regulatory control to screen and quantify chloramphenicol residues in various muscle tissues on a routine basis. Copyright © 2006 John Wiley & Sons, Ltd." @default.
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- W2090831812 date "2006-01-01" @default.
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- W2090831812 title "Performance characteristics of an analytical procedure for determining chloramphenicol residues in muscle tissue by gas chromatography–electron capture detection" @default.
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- W2090831812 doi "https://doi.org/10.1002/bmc.599" @default.
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