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- W2090846210 abstract "In this paper, the optimization of typical reaction variables for a pilot scale synthesis of carbon nanofibers (CNFs) using a fixed-bed reactor has been carried out to provide a more economically viable large scale production of these materials. Using a Ni/SiO2 catalyst (10 wt % Ni) and ethylene as the carbon source, the optimum value of temperature, space velocity, and H2/C2H4 ratio (v/v) in terms of carbon yield was 600 °C, 10000 h−1, and 1:4, respectively. The modification of these variables caused a significant change in the type and amount of solid carbon recovered. Carbon product characterization demonstrated that CNFs with mesoporous character, large external surface, and good thermal stability and crystallinity were obtained. Finally, results demonstrated a successful scale-up by a factor of 45 in the pilot plant scale; a CNFs yield of 106 gCNFs/gcatalytic metal could be obtained at optimal conditions during a reaction time of 60 min at optimal conditions in the pilot plant scale. For the same reaction conditions, only 80 gCNFs/gcatalytic metal were obtained in the laboratory reactor." @default.
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- W2090846210 date "2009-07-31" @default.
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- W2090846210 title "Pilot Plant Scale Study of the Influence of the Operating Conditions in the Production of Carbon Nanofibers" @default.
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- W2090846210 doi "https://doi.org/10.1021/ie9005386" @default.
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