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- W2090963506 abstract "A sensitive method was developed for the determination of deuterated and non-deuterated 1-methyl-1,2,3,4-tetrahydro-β-carboline by combined capillary gas cheomatography and negative-ion chemical ionization mass spectrometry. 1-Methyl-1,2,3,4-tetrahydro-β-carboline was converted into a trifluoroacetyl derivative after pretreatment with fluorescamine and extraction with ethyl acetate. The derivative was separated by capillary gas chromatography and determined by selected-ion monitoring. In the determination, [3,3,4,4- 2 H 4 ]-1-methyl-1,2,3,4-tetrahydro-β-carboline was used as an internal standard. The method developed in this work was used for the determination of deuterated and non-deuterated 1-methyl-1,2,3,4-tetrahydro-β-carboline in human urine samples collected before and after administration of [3,3- 2 H 2 ]- l -tryptophan." @default.
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- W2090963506 title "Highly sensitive method for the determination of 1-methyl-1,2,3,4-tetrahydro-β-carboline using combined capillary gas chromatography and negative-ion chemical ionization mass spectrometry" @default.
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- W2090963506 doi "https://doi.org/10.1016/s0378-4347(00)82357-9" @default.
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