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• W2090986263 abstract "The complexation behaviour of the bidentate ligand tetrakis(O-isopropyl)methylenediphosphonate (L = (iPrO)2P(O)CH2P(O)(OiPr)2) with lanthanide ions has been studied by using triflates Ln(OTf)3 (Ln = La, Pr, Nd) as sources of the Ln3+ cations. At the 2:1 L:Ln stoichiometric ratio, adducts of composition [Ln(OTf)3(L)2(OH2)2] were isolated (Ln = La, Pr, Nd). In the X-ray structure of the cationic [Nd(OTf)2(L)2(OH2)2](OTf), the two coordinated triflates are monodentate. Finally, at higher L/Ln ratios, complexes were difficult to isolate because of a high degree of solvation, but, in one instance, with Ln = La, by using inert atmosphere techniques, the tripositive complex [La(L)4](OTf)3(CH3CN)3 has been obtained and characterised by X-ray. By contrast, in the crystal structures of [Ln(NO3)3(L)2](CH3CN)2, (Ln = Ce, Pr, Nd), all three nitrates are bidentate." @default.
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• W2090986263 date "2005-03-01" @default.
• W2090986263 modified "2023-10-16" @default.
• W2090986263 title "Lanthanide complexes with a chelating methylenediphosphonate" @default.
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• W2090986263 doi "https://doi.org/10.1016/j.poly.2005.01.001" @default.
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