Matches in SemOpenAlex for { <https://semopenalex.org/work/W2090986667> ?p ?o ?g. }
Showing items 1 to 98 of
98
with 100 items per page.
- W2090986667 endingPage "945" @default.
- W2090986667 startingPage "945" @default.
- W2090986667 abstract "Vapour generation inductively coupled plasma optical emission spectrometry (VG-ICP-OES) was used for the determination of the iodine content in milk samples. Modified alkaline ashing of the milk sample was employed for the total digestion of organic matrix constituents. A mixture of potassium hydroxide (2 mL, 2 mol L−1 in ethanol) and calcium nitrate (2 mL, 0.4 mol L−1 in ethanol) was used in the digestion step as an ashing aid for 2 ml of milk sample (or 200 mg of milk powder). Sample ash was then treated with hydrochloric acid (1.5 mL, 5 mol L−1) and sodium sulfite (1.25 mL, 1 mol L−1) for the elimination of carbonates, which would otherwise cause spectral interference. The vapour of elemental iodine was generated by means of oxidation of iodide by hydrogen peroxide (1 mol L−1) in sulfuric acid (5 mol L−1). Using a gas phase separator, matrix elements were completely eliminated; thus the spectral interference of phosphorus (178.222 nm) was removed and the most intense analytical line of iodine (178.218 nm) could be used for determination. The accuracy of the method was verified by analysis of CRM Non-Fat Milk Powder 1549 from NIST, as well as by the comparative study of VG-ICP-OES and ICP-MS results after alkaline solubilization (TMAH 2.5 mL, 10%). The limit of detection for the VG-ICP-OES method is 20 μg L−1 for original milk samples (based on 3σ of blank value). The concentration of iodine in real milk samples was found in the range 0.2–0.8 mg L−1 with a precision of determination from 0.5 to 3.5% (3 replicates)." @default.
- W2090986667 created "2016-06-24" @default.
- W2090986667 creator A5042497740 @default.
- W2090986667 creator A5058832360 @default.
- W2090986667 creator A5073501400 @default.
- W2090986667 creator A5077811179 @default.
- W2090986667 date "2005-01-01" @default.
- W2090986667 modified "2023-09-25" @default.
- W2090986667 title "Vapour generation inductively coupled plasma optical emission spectrometry in determination of total iodine in milk" @default.
- W2090986667 cites W101623866 @default.
- W2090986667 cites W1973064905 @default.
- W2090986667 cites W1975137994 @default.
- W2090986667 cites W1977675716 @default.
- W2090986667 cites W1997801539 @default.
- W2090986667 cites W1998392204 @default.
- W2090986667 cites W2009792885 @default.
- W2090986667 cites W2017977075 @default.
- W2090986667 cites W2032983284 @default.
- W2090986667 cites W2063525702 @default.
- W2090986667 cites W2064395063 @default.
- W2090986667 cites W2072805016 @default.
- W2090986667 cites W2080317929 @default.
- W2090986667 cites W2085594998 @default.
- W2090986667 cites W2087507437 @default.
- W2090986667 cites W2092164696 @default.
- W2090986667 cites W2119388467 @default.
- W2090986667 cites W2142342414 @default.
- W2090986667 cites W2154981493 @default.
- W2090986667 doi "https://doi.org/10.1039/b504525h" @default.
- W2090986667 hasPublicationYear "2005" @default.
- W2090986667 type Work @default.
- W2090986667 sameAs 2090986667 @default.
- W2090986667 citedByCount "28" @default.
- W2090986667 countsByYear W20909866672012 @default.
- W2090986667 countsByYear W20909866672013 @default.
- W2090986667 countsByYear W20909866672014 @default.
- W2090986667 countsByYear W20909866672016 @default.
- W2090986667 countsByYear W20909866672021 @default.
- W2090986667 crossrefType "journal-article" @default.
- W2090986667 hasAuthorship W2090986667A5042497740 @default.
- W2090986667 hasAuthorship W2090986667A5058832360 @default.
- W2090986667 hasAuthorship W2090986667A5073501400 @default.
- W2090986667 hasAuthorship W2090986667A5077811179 @default.
- W2090986667 hasConcept C113196181 @default.
- W2090986667 hasConcept C119128265 @default.
- W2090986667 hasConcept C121332964 @default.
- W2090986667 hasConcept C13965031 @default.
- W2090986667 hasConcept C147789679 @default.
- W2090986667 hasConcept C178790620 @default.
- W2090986667 hasConcept C179104552 @default.
- W2090986667 hasConcept C185592680 @default.
- W2090986667 hasConcept C2777436746 @default.
- W2090986667 hasConcept C2778199549 @default.
- W2090986667 hasConcept C2778562268 @default.
- W2090986667 hasConcept C43617362 @default.
- W2090986667 hasConcept C539932907 @default.
- W2090986667 hasConcept C62520636 @default.
- W2090986667 hasConcept C82706917 @default.
- W2090986667 hasConcept C95974651 @default.
- W2090986667 hasConcept C99293441 @default.
- W2090986667 hasConceptScore W2090986667C113196181 @default.
- W2090986667 hasConceptScore W2090986667C119128265 @default.
- W2090986667 hasConceptScore W2090986667C121332964 @default.
- W2090986667 hasConceptScore W2090986667C13965031 @default.
- W2090986667 hasConceptScore W2090986667C147789679 @default.
- W2090986667 hasConceptScore W2090986667C178790620 @default.
- W2090986667 hasConceptScore W2090986667C179104552 @default.
- W2090986667 hasConceptScore W2090986667C185592680 @default.
- W2090986667 hasConceptScore W2090986667C2777436746 @default.
- W2090986667 hasConceptScore W2090986667C2778199549 @default.
- W2090986667 hasConceptScore W2090986667C2778562268 @default.
- W2090986667 hasConceptScore W2090986667C43617362 @default.
- W2090986667 hasConceptScore W2090986667C539932907 @default.
- W2090986667 hasConceptScore W2090986667C62520636 @default.
- W2090986667 hasConceptScore W2090986667C82706917 @default.
- W2090986667 hasConceptScore W2090986667C95974651 @default.
- W2090986667 hasConceptScore W2090986667C99293441 @default.
- W2090986667 hasIssue "9" @default.
- W2090986667 hasLocation W20909866671 @default.
- W2090986667 hasOpenAccess W2090986667 @default.
- W2090986667 hasPrimaryLocation W20909866671 @default.
- W2090986667 hasRelatedWork W121174007 @default.
- W2090986667 hasRelatedWork W1964387808 @default.
- W2090986667 hasRelatedWork W1970133124 @default.
- W2090986667 hasRelatedWork W1992244075 @default.
- W2090986667 hasRelatedWork W2145492939 @default.
- W2090986667 hasRelatedWork W2319351455 @default.
- W2090986667 hasRelatedWork W2352527736 @default.
- W2090986667 hasRelatedWork W2384823439 @default.
- W2090986667 hasRelatedWork W2391712754 @default.
- W2090986667 hasRelatedWork W3008819105 @default.
- W2090986667 hasVolume "20" @default.
- W2090986667 isParatext "false" @default.
- W2090986667 isRetracted "false" @default.
- W2090986667 magId "2090986667" @default.
- W2090986667 workType "article" @default.