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• W2091082492 abstract "Enyne photocycloaddition with a 2-pyridone yields a mixture of products including amide-bridged 1,2,5-cyclooctatrienes, the first examples of enyne [4 + 4] adducts. Four regio- and stereochemical isomers of the [4 + 4] adduct are possible. All appear to be too strained to be isolated, but they have been identified as their [2 + 2] cyclobutane dimers. Cyclobutane and cyclobutene adducts have also been isolated, [2 + 2] addition products possibly related to the unstable [4 + 4] adducts via Cope rearrangement. Calculations suggest that [3,3] rearrangements have high energy barriers, however, making thermal interconversion unlikely." @default.
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• W2091082492 date "2010-07-15" @default.
• W2091082492 modified "2023-10-18" @default.
• W2091082492 title "Enyne [4 + 4] Photocycloaddition: Bridged 1,2,5-Cyclooctatrienes" @default.
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• W2091082492 doi "https://doi.org/10.1021/ol1014174" @default.
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