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- W2091158085 abstract "Aluminum was incorporated into the mesoporous framework of ethane−silica by one-pot condensation of Al(OiPr)3 with 1,2-bis(trimethoxysilyl)ethane using octadecyltrimethylammonium chloride as surfactant. Powder X-ray diffraction patterns, nitrogen sorption analysis, and TEM results reveal the formation of an ordered mesoporous material with uniform porosity. 27Al MAS NMR confirms the incorporation of aluminum in the framework. The synthesized materials exhibit extremely high hydrothermal stability in boiling water (no obvious change of mesostructure and textural properties was observed even after refluxing in water for 100 h), which could be mainly contributed to the ethane-bridged mesoporous framework. The aluminum-containing mesoporous ethane−silicas are efficient catalysts for the alkylation of 2,4-di-tert-butylphenol by cinnamyl alcohol to yield a flavan." @default.
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- W2091158085 date "2004-05-07" @default.
- W2091158085 modified "2023-09-23" @default.
- W2091158085 title "Hydrothermal Stability and Catalytic Activity of Aluminum-Containing Mesoporous Ethane−Silicas" @default.
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- W2091158085 doi "https://doi.org/10.1021/jp040124o" @default.
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