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- W2091208208 abstract "An ion chromatographic method was developed for the fully automated routine clinical determination of urinary free catecholamines noradrenaline, adrenaline and dopamine with an internal standard (3,4-dihydroxy-benzylamine). Simultaneous clean-up and separation of the analytes are achieved by an on-line purification step and a column-switching technique. The whole procedure requires 45 min. Both the prepurification microcolumn and the analytical column contain cation exchangers. Electrochemical detection was optimized with two working electrodes set at +500 mV for the cleaning step, and +700 mV for detection. Analytical recoveries for all three catecholamines were 90–95% and the detection limits (signal-to-noise ratio = 3) were 5.0, 10.0 and 10.0 pg for noradrenaline, adrenaline and dopamine, respectively." @default.
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- W2091208208 date "1994-06-01" @default.
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- W2091208208 title "Determination of catecholamines by ion chromatography and electrochemical detection" @default.
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- W2091208208 doi "https://doi.org/10.1016/0021-9673(94)80248-3" @default.
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