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• W2091229487 abstract "We have used a fast, sensitive and efficient method for the analysis of volatile carbonyl compounds (saturated aliphatic and unsaturated aldehydes) based on solid-phase microextraction with on-fibre derivatisation. Pentafluorophenylhydrazine was absorbed onto a poly(dimethylsiloxane)/divinylbenzene-coated fibre and exposed to the vapours of aldehyde-containing matrices. The hydrazones formed on the fibre were desorbed into the gas chromatograph injection port and quantified by means of electron-capture detection with high sensitivity (10–90 fmol) and good reproducibility (RSD<10%). The method was applied to the headspace-sampling of volatile carbonyl compounds released during the thermally-induced degradation of sunflower oil." @default.
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• W2091229487 date "2000-07-01" @default.
• W2091229487 modified "2023-10-15" @default.
• W2091229487 title "Solid-phase microextraction with on-fibre derivatisation applied to the analysis of volatile carbonyl compounds" @default.
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• W2091229487 doi "https://doi.org/10.1016/s0021-9673(00)00479-9" @default.
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