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- W2091229703 abstract "2H-NMR stimulated echo experiments have been performed in order to study the molecular basis of the ?-process in viscous glycerol near its glass transition temperature. Decay functions following modified Jeener-Broekaert pulse sequences were compared with predictions from different models for molecular reorientation. Rotational diffusion, rotational random jumps, rotational fixed-angle jumps and combinations of diffusive and jump motions have been tested. All data are fitted with a log-Gaussian distribution of correlation times. Thereby, small-but finite-angle reorientation processes turn out to dominate in the 10-3 s.. 100 s regime. Pure large-angle rotational jumps can be ruled out with high significance. The mean rotational correlation time, ?c, agrees with results from other relaxation experiments which monitor the ?-process of the glass transition." @default.
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- W2091229703 date "1990-10-01" @default.
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- W2091229703 title "<sup>2</sup> H-NMR-Stimulated Echo Study of Ultraslow Reorientational Motion in Viscous Glycerol near Its Glass Transition Temperature" @default.
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- W2091229703 doi "https://doi.org/10.1209/0295-5075/13/3/011" @default.
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