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• W2091229760 abstract "3,4-Dimethoxypropiophenone (3,4-DMPP) is of considerable commercial importance due to its use in fine chemical and drug industries. 3,4-DMPP is traditionally produced by the Friedel–Crafts propionylation of veratrole using homogeneous catalysts which are highly polluting. Zeolites have also been used but they are known to deactivate rapidly. A variety of novel solid acid catalysts such as UDCaT-4 (persulfated alumina zirconia on hexagonal mesoporous silica, HMS), UDCaT-5 (superacidic modified sulfated zirconia) and UDCaT-6 (modified sulfated zirconia nanoparticles on HMS) were synthesized in our laboratory and characterized. Amongst them UDCaT-5 was the most active and selective. The current work deals with development of clean and benign route for 3,4-DMPP synthesis using UDCaT-5 as catalyst in the absence of any solvent. Effects of various parameters were studied in order to optimize the conversion of veratrole and selectivity to 3,4-DMPP. Based on the experimental data a suitable mathematical model was developed to represent the reaction kinetics." @default.
• W2091229760 created "2016-06-24" @default.
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• W2091229760 date "2012-01-01" @default.
• W2091229760 modified "2023-10-01" @default.
• W2091229760 title "Friedel–Crafts propionylation of veratrole to 3,4-dimethoxypropiophenone over superacidic UDCaT-5 catalyst" @default.
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• W2091229760 doi "https://doi.org/10.1016/j.apcata.2011.10.027" @default.
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