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• W2091241306 abstract "A mL-scale continuous crystallizer has been newly developed to produce small crystals with a narrow size distribution. The crystallizer is used for the poor solvent crystallization of glycine and L-alanine. The crystallizer is composed of a stainless-steel mixing vessel with an inner volume of 0.9 mL and a high-speed agitator that can agitate the crystallization solution up to 24,000 rpm. Glycine or L-alanine aqueous solution and poor solvent (methanol) are supplied into the vessel at a constant flow rate and intensely mixed by the agitator. The average residence time was set at 0.33, 3.3 and 33 s by changing the flow rate of an amino acid solution and poor solvent. The crystals obtained by the crystallizer are small and uniform in size, comparing with those obtained by a conventional beaker-scale semi-batch and continuous MSMPR type crystallizers. For example, glycine crystals having the 1/38 of the size of crystals obtained by a semi batch crystallizer were obtained. The short residence time that can be attained by the present mL-scale crystallizer is advantageous for the production of small crystals with a narrow size distribution. The size distribution can be further controlled by changing the mixing ratio of poor solvent." @default.
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• W2091241306 date "2012-01-01" @default.
• W2091241306 modified "2023-09-27" @default.
• W2091241306 title "Control of Crystal Size Distribution Using a mL-Scale Continuous Crystallizer Equipped with a High Speed Agitator" @default.
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• W2091241306 doi "https://doi.org/10.1252/jcej.11we158" @default.
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