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- W2091275013 abstract "Abstract The trifluoroacetates of 52 stereoisomeric alcohols were prepared and their 19F-NMR shifts were determined in different solvents. In dimethylsulfoxide equatorial trifluoroacetate groups are generally more deshielded than axial groups, which is reversed in most cases in carbon tetrachloride. This effect is discussed in terms of intramolecular hydrogen bonding. The differences between endo and exo trifluoroacetates of bicyclic alcohols did not follow a simple pattern. The conformational equilibria of some cyclohexane trifluoroacetates were determined with the aid of both line width and shifts of the X proton in the NMR spectra." @default.
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- W2091275013 date "1970-01-01" @default.
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- W2091275013 title "19F-NMR shifts and conformations of cyclic and bicyclic trifluoroacetates" @default.
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- W2091275013 doi "https://doi.org/10.1016/s0040-4020(01)98746-0" @default.
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