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- W2091400814 abstract "Abstract The mechanism of methane reforming with carbon dioxide over 1.0 wt.% Rh/SBA-15 catalyst has been studied by the 13 C and 1 H magic-angle spinning (MAS) NMR spectroscopies under controlled atmosphere condition using 13 CH 4 + 12 CO 2 and 12 CH 4 + 13 CO 2 as reactants. The effect of temperature in the region of 298–1023 K on the reaction was investigated and the contents of various 13 C and 1 H species were obtained quantitatively by the NMR technique. When treated at 573 K, the carbon exchange between methane and carbon dioxide can be observed. With the temperature rising to 773 K, the adsorbed CH 3 O* species is formed but no reforming reaction occurs. In the high temperature range of 873–1023 K, the reforming reaction was observed with concomitant appearance of the adsorbed CH 2 O* species and the intensity of both CH 3 O* and CH 2 O* increases with increasing temperature, indicating that the decomposition of CH 3 O* to CH 2 O* occurs and the products of dry reforming are formed from decomposition of the adsorbed CH 2 O* species." @default.
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- W2091400814 date "2011-07-01" @default.
- W2091400814 modified "2023-10-18" @default.
- W2091400814 title "Controlled atmosphere 13C and 1H MAS NMR study of reforming route of methane with carbon dioxide over Rh/SBA-15" @default.
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- W2091400814 doi "https://doi.org/10.1016/j.apcata.2011.05.004" @default.
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