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- W2091698712 abstract "The 7Li NMR spectrum for polycrystalline lithium nitride has been examined as a function of both temperature and magnetic field. Two central m=½ to m=—½ transitions and two pairs of m=±32 to m=±½ satellite transitions have been observed; these results are consistent with the presence of the two nonequivalent lithium sites in the known crystal structure of Li3N. The quadrupole coupling constants for the two lithium sites, as determined from the frequency separation of the satellite transitions, are 288±4 and 584±6 kc/sec at room temperature. These values are in good agreement with those determined from the field dependence of the second-order quadrupolar widths of the two m=½ to m=—½ transitions. The central transitions have been examined as a function of temperature at a resonant frequency of 16 Mc/sec, where the linewidth is determined primarily by dipolar effects. As the temperature is increased from 77°K, the linewidths remain relatively constant at low temperatures but narrow abruptly between roughly −75°C and room temperature. The observed narrowing is attributed to the diffusion of lithium ions." @default.
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- W2091698712 date "1966-09-01" @default.
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- W2091698712 title "NMR Studies of<sup>7</sup>Li in Polycrystalline Lithium Nitride" @default.
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- W2091698712 doi "https://doi.org/10.1063/1.1727796" @default.
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