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- W2091763290 abstract "A new synthetic route for the preparation of the alkyl esters of 1,2-benzisothiazoline-3-acetic acid 1,1-dioxide (III) is described in this paper. In attempts to prepare the alkyl esters of ortho-sulfamoylcinnamic acid (II) by the procedure of Leov and Kormendy, the authors observed that the compounds obtained were not the expected cinnamic acid derivatives (II), but the derivatives of 1,2-benzisothiazoline (III). The 1,2-benzisothiazoline derivatives (III) are believed to have formed as a result of an intramolecular rearrangement of the cinnamates (II) by a mechanism similar to the Michael reaction. Proof of the chemical structures is provided by UV, IR, NMR, and X-ray crystallographic studies. Six compounds were synthesized and tested for antielectroshock activity in addition to a general pharmacological screening. One compound showed a slight antielectroshock activity in mice, but in general, the compounds did not possess any significant pharmacological activity." @default.
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- W2091763290 date "1969-05-01" @default.
- W2091763290 modified "2023-09-23" @default.
- W2091763290 title "Novel Synthesis of Some 1, 2-Benzisothiazoline Derivatives: Cyclization of ortho-Sulfamoylcinnamates by the Michael Reaction" @default.
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- W2091763290 doi "https://doi.org/10.1002/jps.2600580528" @default.
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